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Fractions from the above fractionation were dissolved with solvent A (0.1% formic acid in H 2 O) and separated with a homemade reversed-phase 25-cm analytical column (75 ΞΌm ID, 1.9 ΞΌm C18) in a 65-min gradient from 5% to 50% solvent B (0.1% formic acid in 80% ACN) using the EASY-nLC 1200 system (Thermo Fisher Scientific)
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